NMR Facility
Chemistry Department NMR Research Facility
Open Access NMR Experiment Lists
The tables below summarises the experiments available through the fully automated open-access NMR spectrometers situated close to the organic synthetic laboratories. A greater range of experiments are available for trained users through use of the bookable spectrometers.
Experiments available on the DPX200 NMR spectrometer:
Experiment |
Description |
Range (ppm) |
Number of transients |
Run time (min:sec) |
N CRL_PROTON |
1H (proton) |
16 → -4 |
16 |
1:32 |
N CRL_PROTON_WIDE |
1H (wide SW) |
30 → -10 |
16 |
1:32 |
Experiments available on the AVF400, AVH400 and AVG400 NMR spectrometers:
Experiment |
Description |
Range (ppm) |
Number of transients |
Run time (approx, min: sec) |
Night time? |
|---|---|---|---|---|---|
N CRL_PROTON |
1H (proton) |
16 → -4 |
16 |
1:32 |
|
N CRL_PROTON_WIDE |
1H (wide SW) |
30 → -10 |
16 |
1:32 |
|
N CRL_PROTON_QUANT |
1H (quantitative) |
16 → -4 |
4 |
2:26 |
|
N CRL_PROTON_ESPE |
1H (solvent suppression using the excitation sculpting with perfect echo) |
12 → -3 |
8 |
1:26 |
|
N CRL_FLUORINE |
19F (1H coupled) |
0 → -250 |
16 |
0:48 |
|
N CRL_FLUORINE_HDEC |
19F (1H decoupled) |
0 → -250 |
16 |
0:48 |
|
N CRL_FLUORINE_QUANT |
19F (1H coupled, quantitative) |
0 → -250 |
4 |
2:02 |
|
N CRL_FLUORINE_QUANT_HDEC |
19F (1H decoupled, quantitative) |
0 → -250 |
4 |
2:02 |
|
n CRL_FLUORINE_LONG |
19F (1H coupled, long) |
0 → -250 |
256 |
11:40 |
Yes |
N CRL_PHOSPHORUS |
31P (1H coupled) |
0 → -250 |
16 |
0:54 |
|
N CRL_PHOSPHORUS_HDEC |
31P (1H decoupled) |
100 → -100 |
16 |
0:54 |
|
N CRL_PHOSPHORUS_QUANT |
31P (1H coupled, quantitative) |
100 → -100 |
4 |
2:04 |
|
N CRL_PHOSPHORUS_QUANT_HDEC |
31P (1H decoupled, quantitative) |
100 → -100 |
4 |
2:04 |
|
n CRL_PHOSPHORUS_LONG |
31P (1H coupled, long) |
100 → -100 |
256 |
13:01 |
Yes |
N CRL_ALUMINIUM |
27Al (1H coupled) | 250 → -50 | 256 | 2:10 | |
n CRL_CARBON |
13C (1H decoupled) |
225 → -25 |
256 |
14:33 |
Yes |
n CRL_CARBON_DEPTQ |
13C DEPTQ (1H decoupled, CH/CH3 positive, C/CH2 negative) |
225 → -25 |
256 |
14:44 |
Yes |
n CRL_COSY |
1H-1H COSY |
11 → -1 |
1 |
5:07 |
Yes |
n CRL_HSQCED |
1H-13C HSQC (multiplicity edited) |
1H: 11 → -113C: 182 → -2 |
2 |
10:02 |
Yes |
n CRL_HMBC |
1H-13C HMBC |
1H: 15 → -513C: 224 → -45 |
2 |
31:55 |
Yes |
n CRL_NOESY |
1H-1H NOESY |
11 → -1 |
4 |
24:00 |
Yes |
Note if no day-time experiments are queued to run, night-time experiments (excluding HMBC and NOESY) will run during the day-time.